How to collect a Nuclear Magnetic Resonance (NMR) spectrum?

I wanted to find a way to detect Phosphorus in an organic compound or substance (like blood) Is a NMR spectrum a way to do this? If so, how? If not, then what is?

Any help is appreciated, thanks!

PS. I saw this question: http://answers.yahoo.com/question/index?qid=200901... but there's no information as to how to collect the spectrum.

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